ABSTRACT : This research aims to determine the levels of lead (II) and lead (IV) metal ion species by potentiometric methods using concentration cells and study the distribution of lead (II) and lead (IV) metal ions in the waters of Teluk Gelam Lake. The results showed the linear regression equation for metal ion of lead (II) y = 4.9162x+0.4 while lead (IV) y = 6.1105x+0.88 with R2 values 0.999…