Tempurung kelapa merupakan sisa biomassa yang terdiri dari lignin, selulosa dan hemiselulosa, memiliki potensi sebagai bahan baku dalam sintesis oksida grafena tersulfonasi (S-GO). S-GO disintesis menggunakan metode Hummer dengan asam sulfat sebagai agen sulfonasi. Hasil sintesis meliputi grafit, oksida grafena, dan oksida grafena yang telah tersulfonasi. Karakterisasi FTIR digunakan untuk meng…
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Fagraea fragrans is a plant commonly found in Sumatera island. Several studies reported that F. fragrans has various pharmacological activities indicating the presence of active compounds in this plant, such as phenolics dan flavonoids. Hence, This study aims to estimate the total phenolic and flavonoid content, determine the antioxidant activity, and identify the compounds with LC-MS. The rese…
Sungkai belongs to the Lamiaceae famili with the latin name Peronema canescens Jack. Sungkai leaves have traditionally been used as a medicine to increase the body’s immune system. Its efficacy as an immune system drug is related to the presence of antioxidant. The aims of this research to determine the antioxidant activity of the ethyl acetate fraction of sungkai leaves (P. canescens Jack.) …
Ludwigia octovalvis belongs to Ludwigia genus from family of Onagraceae. Some bioactivities from extract of this plant had been reported such as antioxidant and antidiabetic. The antioxidant activity from the leaves and stem of L. octovalvis extract have been reported. Previous studies have been successfully isolated methyl gallate and quercetin from L. octovalvis fruit.Meanwhile, the antioxida…
VCO is an oil obtained from fresh old coconut flesh squeezed with or without the addition of water, without heating, or by heating less than 60°C. The main component of VCO is medium-chain fatty acids, especially lauric acid. Over time, there have been various technologies for making VCO, but pre-existing methods still have weaknesses, namely that the yield produced is still low and the qualit…
Virgin coconut oil adalah minyak yang dihasilkan dari pati kelapa yang telah diproses secara higienis dan tanpa pemurnian kimia, sehingga kandungan yang penting dalam minyak tetap dipertahankan. VCO umumnya dibuat dengan menggunakan dua metode diantaranya metode kering dan metode basah. Salah satu pembuatan VCO dengan metode basah adalah elektrolisis. Metode elektrolisis dilakukan dengan mengal…
Ibu menyusui yang terpapar asap rokok dapat terkontaminasi nikotin, terutama pada ASI yang dihasilkan oleh Ibu menyusui. Penelitian ini bertujuan untuk memvalidasi metode analisis kadar nikotin dalam ASI dengan metode GLC serta menentukan dan membandingkan kadar nikotin dalam ASI ibu perokok pasif yang sedang menyusui berdasarkan lamanya terpapar (1-15 tahun). Validasi metode dilakukan dengan m…
Flacourtia rukam is one of the traditional medicinal plants used in the treatment of various diseases. The disease can be caused by various factors, one of which is due to free radicals. Antioxidant compounds are scientifically known to be able to inhibit free radicals. This research was conducted to test the antioxidant activity of the ethyl acetate fraction of F. Rukam twigs. The extraction u…
Semprawang (Dillenia ochreata) is a plant that belongs to the Dilleniaceae family. D. ochreata is empirically used by the Musi as a cure for scabies. Information about the activity of D.ochreata is still very limited. The purpose of this study was to determine the antioxidant and anticholesterol activity of the stem bark of Semprawang (Dillenia ochreata). The extraction method used is the maser…
Isolation of secondary metabolite from n-hexane extract of the stem of Tinospora crispa had been done. The extraction was done by maceration. The extract of n-hexane was separated and purified by chromatography column techniques. Antioxidant activity of the isolated compound was conducted by DPPH (1.1-diphenylpycryl hidrazyl) method with concentration variation of 1000, 500, 250, 125, 62.5, 31.…
It has been done the research about “The Characteristic Mixtures Biodiesel From Ketapang Seed Oil (Terminalia catappa Linn) With Solar Using NaOH Catalyst“. The purpose of research is to determine the optimum condition blending biodiesel from ketapang seed oil with solar. Biodiesel 0%, 5%, 15%, 25%, 35%, 45%, 55%, 65%, 75%, 85%, 95%, 100% which characterized by using method of ASTM (America…
Isolation of flavonoid compound has been done from ethyl acetate fraction of Calophyllum pulcherrimum leaves. Extraction conducted by partition method using ethyl acetate and resulted compound was separated using chromatography technique. Product isolation is 11 mg yellow powder with melting point 281-282°C. 13C-NMR DEPT 135° dan DEPT 90° spectrum showed isolation compound have 27 atom carbo…
It has been done the research kinetics of oxidation reactions ketapang seed oil (Terminal ia catappa Linn) and antioxidant effects of the addition BHT to the peroxide number. The purposes of the research were to define the influence of the addition of antioxidants BHT to long the storage, the kinetics of oxidation reactions ketapang seed oil, and determine the content of seed oil fatty acids ke…
Oxidation of the hydroxyl group (C-3 -OH) of ursolic acid [oleanolic acid], isolated from methanolic extract of tembesu fruit, had been done using Jones’ reagent (C1O3/H2SO4/H2O) in acetone with 40% yield. Spectrum data of ]H-NMR showed that the methine proton at C-3 position of the triterpenoids was no longer existed, and the analysis of mass spectrum showed that the oxidation products had m…
The phenolic compound have been isolated and characterizated from ethyl acetate extract of stem bark of Garcinia sizygiifolia. The extraction was done by maseration. Separation and purification were done by column chromatography. The isolated compound was a yellow solids with melting point 243°C-245°C. The structure of this compound was determined based on spectral data including IR, UV, NMR …
Preparation of nanomaterial based on polyoxometalate with Si02, Ti02, ZrOCl2 and TaCI to form nanomaterial H4[a-SiWi204o]-nH20-Si02, H4[a-SiWi2O40].nH2O-TiO2, H4[a-SiW,2O40].nH2O-ZrOCl2 and H4[a-SiWi2O40].nH2Ota has been carried out. Nanomaterials were characterized using FT-IR, XRD and SEM. The results of characterization show that nanomaterials ELt[a-SiWi204o].nH20-Si02 and nanomaterial from …
The Influence Of Glucose Composition And Montmorilonite Toward The Caracteristic Of Composite Catalyst Montmorilonite Carbon Sulfonate Penelitian pengaruh komposisi glukosa dan montmorilonit terhadap sifat katalis komposit montmorilonit karbon sulfonat telah dilakukan. Katalis komposit montmorilonit karbon sulfonat (M-CS) dibuat dengan cara mencampurkan montmorilonit dan glukosa sampai homogen …
Preparation of calcium oxide from Portunus pelagicus through thermal decomposition for 3 hours at various temperature 700 °C, 800 °C, 900 °C, 1000 °C, and 1100 °C. The calcium oxide from decomposition was carried out and characterized by X-Ray Diffractometer (XRD), FT-IR spectrophotometer and SEM-EDX analyses. The result of XRD show decomposition Portunus pelagicus at 1000 °C have diffrac…
Conversion of cyclohexanone to produce adipic acid via oxidation reaction by H2O2 with natural mineral catalysts (zeolite and bentonite) has been carried out. Catalysts zeolite and natural bentonite before and afiter reaction characterized using spectrophotometer FT-IR and difractometer X-ray. Product of conversion was characterized through the determination of melting point, identification usi…
The research by title effect of the differences hydrotermal extraction methods and calcination the characterization of silika from corn cob has been performed. Corncob is extracted by hydrothermal variation NaOH concentration methods 0.5;1.0; 1.5 and 2.0 M and calcination methods with temperature variations 600, 700 and 800oC, to obtain silica powder and on hydrothermal methods with NaOH concen…
The Effect of 2-Propanol Solvent Volume in Electrodes Making Using the Doctor Blade Method on the Performance of the Membrane Electrode Assembly (MEA) in Direct Ethanol Fuel Cell (DEFC) Mohd Hilal Assegaf: Supervised by Dr. Dedi Rohendi, M.T and Fahma Riyanti, M.Si Chemistry, Faculty of Mathematics and Natural Sciences, Sriwijaya University xi + 61 pages, 4 tables, 8 pictures, 4 appendices Stud…
Telah dilakukan penelitian tentang preparasi dan karakterisasi ZnO dan ZnO/bentonit dan aplikasinya untuk adsorpsi Cr(VI). Bentonit sebelum diaplikasikan perlu diaktivasi terlebih dahulu. Proses aktivasi dilakukan dengan penambahan asam sulfat (H2SO4) dan kemudian dilakukan pencucian sampai pH 5. Kation pada bentonit akan dipertukarkan dengan oksida logam ZnO. Bentonit teraktivasi, ZnO/bentonit…
Jengkol mistletoe [Scurrula ferruginea (Jack) Danser] is one type of plants from the Loranthaceae group. Mistletoe has secondary metabolites compound in the form of flavonoid, tannin, terpenoid and saponin which has antioxidant activity. This study aims to know fractions that have antioxidant activity, the class of compounds, and IC50 values antioxidant compounds of jengkol mistletoe leaves. Th…
Archidendron jiringa is one of the plant that has the potential as an antihyperlipidemia. Jengkol fruit peel contains phenolic, flavonoid, tannin and saponin chemical compounds that can act as antihyperlipidemia. The purpose of this research is to look at the antihyperlipidemic effect of ethanol extract of jengkol fruit peel to decrease levels of total cholesterol, LDL (Low density lipoprotein)…
Jengkol seed (Archidendron jiringa) contains of secondary metabolite such as flavonoids, alkaloids, tannins, saponins, phenolics and triterpenoids that have the potential as antihyperlipidemia. This study aims to determine the characteristics and effects of ethanol extract of jengkol seeds to decrease total cholesterol, LDL and triglyceride levels. Test animals test are divided into 5 groups wh…
The anti-inflammatory activity of ethanol extract of jengkol seed (Archidendron jiringa) test on carrageenan-induced male white rats has been carried out. The phenolic content in jengkol seed has potential as an inhibiting compound of inflammation. This study aims to determine the total phenolic content of the extract and anti-inflammatory effects based on decreasing the edema volume of carrage…
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Telah dilakukan penelitian analisis radionuklida Cs-137 pada sampel air di7stasiun DAS musi kota Palembang menggunakan spektrometer gamma. Pengaruh karakteristik perairan diantaranya pH air, konduktivitas dan turbiditas masing-masing stasiun terhadap konsentrasi Cs-137 dan menentukan pola penyebaran Cs-137 dengan bantuan software SMS (Surface Water modeling Sistem) dan ArcGIS 10.5. Hasil peneli…
Telah dilakukan preparasi kalsium oksida dari cangkang telur puyuhdengan proses dekomposisi selama 3 jam pada variasi temperatur 600 - 1100°C. Kalsium oksida yang telah dipreparasi dikarakterisasi menggunakan X-Ray Difraktometer (XRD) dan pektrofotometer FT-IR. Hasil analisa XRD menunjukkan pola difraksi CaO pada temperatur 900°C mendekati hasil difraksi CaO standar dari JCPDS yang memiliki n…