Oxidation of the hydroxyl group (C-3 -OH) of ursolic acid [oleanolic acid], isolated from methanolic extract of tembesu fruit, had been done using Jones’ reagent (C1O3/H2SO4/H2O) in acetone with 40% yield. Spectrum data of ]H-NMR showed that the methine proton at C-3 position of the triterpenoids was no longer existed, and the analysis of mass spectrum showed that the oxidation products had m…
Preparation of nanomaterial based on polyoxometalate with Si02, Ti02, ZrOCl2 and TaCI to form nanomaterial H4[a-SiWi204o]-nH20-Si02, H4[a-SiWi2O40].nH2O-TiO2, H4[a-SiW,2O40].nH2O-ZrOCl2 and H4[a-SiWi2O40].nH2Ota has been carried out. Nanomaterials were characterized using FT-IR, XRD and SEM. The results of characterization show that nanomaterials ELt[a-SiWi204o].nH20-Si02 and nanomaterial from …
Preparation of calcium oxide from Portunus pelagicus through thermal decomposition for 3 hours at various temperature 700 °C, 800 °C, 900 °C, 1000 °C, and 1100 °C. The calcium oxide from decomposition was carried out and characterized by X-Ray Diffractometer (XRD), FT-IR spectrophotometer and SEM-EDX analyses. The result of XRD show decomposition Portunus pelagicus at 1000 °C have diffrac…