This research aims to synthesize Fe3O4/activated carbon@NiO composite used in the adsorption and degradation process of Congo red dye. Nanomagnetic Fe3O4 utilized to reduce the band gap value of NiO as well to impart magnetic properties. Activated carbon from bamboo is utilized as an adsorbent in the adsorption process and NiO as a photocatalyst in the degradation process. The Fe3O4/activated c…