Ni0,5Co0,5TiO3 composites with PVA have been synthesized using the solids reaction method by mechanical milling technique and characterized using XRD, SEM-EDS, FTIR, and VNA. The XRD results showed a trigonal structure (R-3) with the lattice parameter increasing from 5.0486 Å to 5.0561 Å as the PVA concentration increased. SEM-EDS confirmed the distribution of homogeneous particles at 10% PVA…